Frank insisted that he was not asleep________ I had great difficulty in waking him up.

A．whether　　

B．a(chǎn)lthough

C．for　　　　

D．so

B解析：句意：盡管我費(fèi)了好大勁才將他叫醒，但弗蘭克堅(jiān)持說他沒有睡熟。although雖然；盡管；whether是否；for因?yàn)�；so因此。根據(jù)句意選B項(xiàng)。

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